978-272-9734
nmrdata@custom-nmr-service.com
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1D 1H, 13C, 31P, 19F spectra
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1D 1H selective decoupling data
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1D NOE
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Variable temperature data, from 5°C to 130°C
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13C DEPT
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2D 1H-1H COSY, 1H-1H NOESY, 1H-1H TOCSY
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2D 1H-13C HSQC, 1H-13C HMBC
With longer turn-around time, we conduct research level data acquisition
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1D spectra of 11B, 29Si, 23Na, or any other NMR active nuclei
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NMR data sets of very limited quantity material (HMBC data with 20 µg of compound with M.W. about 500)
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2D or 3D solution NMR data sets of proteins
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Solid state NMR data
We will also provide data analysis upon request. For example, spectral assignment, J-coupling constant calculation, stereochemistry determination.
Instruments used: Bruker 400MHz AVANCE, Bruker 500MHz AVANCE II. Usage of 600MHz to 900MHz instrument can be arranged when there is a need for it.
Others
We routinely acquire NMR data that a chemist typically needs. They include, but are not limited to
WE WILL PICK UP SAMPLES FROM YOUR LAB, AND RETURN DATA TO YOU THE SAME DAY, SAVING YOU VALUABLE TIME TO CONCENTRATE ON YOUR CHEMISTRY.
Various ligand-protein binding study data, such as STD, waterLOGSY
Data analysis, e.g. spectral assignment, J-coupling constant calculation, conformation determination
Water or multiple solvent suppression 1H data
OUR SERVICES
31P data
Data of other NMR active nuclei, e.g. 29Si, 11B, 195Pt
19F data
qNMR work
1D NOE or 1H with selective decoupling data
1H – 13C 2D HSQC data
1H – 13C 2D long range correlation experiment HMBC data
Variable temperature NMR, range: 5°C to 130°C
13C DEPT data
1H – 1H 2D COSY, NOESY or TOCSY data
1H data
13C data